Nbhp mcgho yncur
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Nbhp mcgho yncur
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Weband R-NBHP were 12.8 min and 13.9 min, respectively. 2.8 Preparative synthesis of S-NBHP The preparative reduction of 1-boc-3-piperidinone was con-ducted at the substrate concentration of 0.5 M in a 20 ml aqueous buffer system containing 1 g recombinant E. coli. Glucose of 2.7 g was added for the NADPH regeneration. The Web5 de may. de 2014 · To our knowledge, there are no published biotransformation methods scalable to prepare S-NBHP. We report here the development of an efficient process catalyzed by recombinant ketoreductase (KRED ...
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Web19 de abr. de 2024 · Asymmetric reduction of N-Boc-piperidin-3-one (NBPO) by reductases is a practical way to produce (S)-NBHP, since it can be carried out under mild reaction conditions, and results in high yield and remarkable enantioselectivity.However, only two cases of biocatalytic approaches were reported. The first practical process towards the …
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